Black Oxide Coating Specifications

Birchwood Technologies Resources

Black Oxide Coating Specifications: AMS2485 & MIL-DTL-13924

AMS2485 and MIL-DTL-13924 are key specifications that define the requirements for black oxide coatings on ferrous alloys and steel. Used extensively in aerospace, defense, and industrial applications, these standards ensure that black oxide finishes provide reliable corrosion resistance, enhanced surface performance, and a uniform appearance.

History and Innovation of Black Oxide

Black oxide coatings have been used since the early 1900s, when workers immersed iron parts into vats of boiling lye at 285-300°F heated over open fires. Despite the risks of handling scalding solutions, the process became widespread, and by the 1930's, black oxide had gained commercial importance. In 1948, the Society of Automotive Engineers (SAE) introduced AMS2485 to standardize the process and establish testing requirements for high-quality coatings.

For decades, the specifications required parts to be treated in boiling aqueous alkali oxidizing baths, even as technological advancements showed that identical coatings could be achieved at much lower temperatures. In 2024, Birchwood Technologies collaborated with the SAE Council to modernize the AMS2485 standard. The updated specification, AMS2485-M, now recommends that time and temperature conditions follow the chemistry manufacturer's guidelines. This change ensures that various formulations can be used effectively while maintaining the required coating quality. By accommodating advancements in chemical processes and supporting innovation, the updated specification remains relevant and inclusive of diverse manufacturing practices.

This update to coating specifications marks a turning point for the black oxide industry, enabling a move away from hazardous boiling caustic baths toward safer, more user-friendly solutions. For over 20 years, Birchwood Technologies has recognized that Tru Temp delivers the same high-quality black oxide coating at just 200°F — and now, the rest of the industry knows it too!

Key Requirements of AMS2485 & MIL-DTL-13924

Both specifications outline similar requirements, including:

  • Uniform Appearance and Quality:
    The coating must be uniformly black or dark gray, free from red oxide spots, and must be smooth, dense, and adherent
  • Coating Integrity:
    Coatings must pass specific tests, such as the oxalic acid test, to evaluate the integrity and durability of the coating.
  • Smut Test:
    Coated parts must be free from reddish-brown or green loose material. This is verified by wiping the coated surface with a clean, white cloth to ensure no discolored residue is present, indicating a clean and high-quality finish.
  • Coating Thickness:
    Black oxide coatings are non-dimensional. Under regulations, they must be under 0.0001" thick, but the coating thickness is in fact approximately 0.00002", or 0.5µm.
Oxalic Acid Test on blackened steel
Oxalic Acid Test on blackened steel. The dark center and lighter edges show this is a good result.

Responsibility of the Process Operator: Certification and Testing

While Tru Temp 2nd Gen is certifiable to all required standards, the operator performing the black oxide process must conduct regular testing and paperwork to officially certify to these standards.

The full AMS2485 specification must be purchased from SAE International.

MIL-DTL-13924 can be downloaded for free.